trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)2]

Base Information

Chemical Name:trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)2]
CAS No.:226948-51-2
Molecular Formula:C₃₂H₄₆N₄Ru
Molecular Weight:587.814
Hs Code.:

trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC<sub>6</sub>H<sub>5</sub>)2]

Synonyms:trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)2]

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Chemical Property of trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)2]

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Technology Process of trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)2]

There total 1 articles about trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 101981-49-1,143059-91-0,293299-17-9
[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₄OCH₃-p)2]

: 536-74-3
phenylacetylene

: 226948-51-2
trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)2]

Guidance literature:: With NaOMe; Zn amalgam; In methanol; N2-atmosphere; addn. of Na metal to soln. of alkyne, addn. of Ru-complexand Zn-Hg, refluxing for 1 h (pptn.); cooling, collection, dissoln. (C6H6), crystn. (difusion of hexane); elem. anal.;
DOI:10.1021/om990009d

Reference yield: 68.0%

: ammonium hexafluorophosphate

: 226948-51-2
trans-[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)2]

: 80937-33-3
oxygen

: 226948-55-6
[Ru(1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)(C*CC₆H₅)(CO)]PF₆

Guidance literature:: In 1,2-dichloro-ethane; bubbling O2 through soln. of Ru-complex and NH4PF6 for 3 h (pptn.); collection (filtration), washing (H2O, Et2O), drying, recrystn. (CH2Cl2:Et2O); elem. anal.;
DOI:10.1021/om990009d