4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol

Base Information

Chemical Name:4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol
CAS No.:485321-79-7
Molecular Formula:C₃₂H₄₂O₂S₂Si
Molecular Weight:550.902
Hs Code.:

4-(<i>tert</i>-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol

Synonyms:4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol

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Technology Process of 4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol

There total 5 articles about 4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 31593-39-2
2-phenethyl-[1,3]dithiane

: 125975-53-3,147220-48-2,116996-54-4
(2S)-O-(tert-butyldiphenylsilyl)-1,2-epoxybutan-4-ol

: 485321-79-7
4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4039(02)02181-0

Reference yield:

: 116996-53-3
Methanesulfonic acid (S)-4-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-butyl ester

: 485321-79-7
4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / K₂CO₃ / methanol / 0 °C

2: 98 percent / n-BuLi / tetrahydrofuran / 20 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4039(02)02181-0

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 485321-79-7
4-(tert-butyl-diphenyl-silanyloxy)-1-(2-phenethyl-[1,3]dithian-2-yl)-butan-2-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / Et₃N; DMAP / CH₂Cl₂ / -10 °C

2: CH₂Cl₂ / 12 h / 20 °C

3: BCl₃ / CH₂Cl₂ / -10 °C

4: 88 percent / K₂CO₃ / methanol / 0 °C

5: 98 percent / n-BuLi / tetrahydrofuran / 20 °C

With dmap; n-butyllithium; boron trichloride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0040-4039(02)02181-0