C₅₂H₅₈N₁₄O₁₂

Base Information

Chemical Name:C₅₂H₅₈N₁₄O₁₂
CAS No.:1310039-81-6
Molecular Formula:C₅₂H₅₈N₁₄O₁₂
Molecular Weight:1071.12
Hs Code.:

C<sub>52</sub>H<sub>58</sub>N<sub>14</sub>O<sub>12</sub>

Synonyms:C₅₂H₅₈N₁₄O₁₂

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Chemical Property of C₅₂H₅₈N₁₄O₁₂

Chemical Property:

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Technology Process of C₅₂H₅₈N₁₄O₁₂

There total 9 articles about C₅₂H₅₈N₁₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₁N₇O₇

: 1310039-80-5
C₂₆H₂₉N₇O₆

: 1310039-81-6
C₅₂H₅₈N₁₄O₁₂

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/ol201184b

Reference yield:

: 1310039-93-0
C₁₅H₂₂N₂O₄

: 1310039-80-5
C₂₆H₂₉N₇O₆

: 1310039-81-6
C₅₂H₅₈N₁₄O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1: iodine; silver trifluoroacetate / chloroform / 15 h / 20 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

4: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran; methanol / 3 h / 20 °C

6: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 16 h / 20 °C

7: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

8: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; iodine; silver trifluoroacetate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; copper(II) sulfate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2: Sonogashira coupling;
DOI:10.1021/ol201184b

Reference yield:

: C₁₄H₂₀N₂O₄

: 1310039-80-5
C₂₆H₂₉N₇O₆

: 1310039-81-6
C₅₂H₅₈N₁₄O₁₂

Guidance literature:: Multi-step reaction with 9 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

2: iodine; silver trifluoroacetate / chloroform / 15 h / 20 °C

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 20 °C

4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

5: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

6: tetrabutyl ammonium fluoride / tetrahydrofuran; methanol / 3 h / 20 °C

7: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 16 h / 20 °C

8: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

9: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; iodine; silver trifluoroacetate; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; copper(II) sulfate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3: Sonogashira coupling;
DOI:10.1021/ol201184b