N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide

Base Information

Chemical Name:N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide
CAS No.:1201640-56-3
Molecular Formula:C₂₅H₃₈N₄O₄
Molecular Weight:458.601
Hs Code.:

Synonyms:N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide

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Chemical Property of N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide

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Technology Process of N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide

There total 7 articles about N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1201640-54-1
3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanoic acid

: 99863-45-3
N-(2,2-dimethoxyethyl)cyclohexanamine

: 1201640-56-3
N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide

Guidance literature:: With 2-propane phosphonic acid anhydride; triethylamine; In tetrahydrofuran; acetonitrile; at 25 ℃; for 0.25h;

Reference yield:

: 1201640-34-7
tert-butyl 3-[2-(3-bromophenyl)ethoxy]propanoate

: 1201640-56-3
N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 0.08 h / 100 °C / Microwave irradiation

2: potassium carbonate / methanol; dichloromethane / 1 h / 25 °C / Inert atmosphere

3: copper(l) iodide; sodium azide / water; tert-butyl alcohol / 6 h / 70 °C / Microwave irradiation

4: trifluoroacetic acid / dichloromethane / 0.5 h / 25 °C

5: 2-propane phosphonic acid anhydride; triethylamine / tetrahydrofuran; acetonitrile / 0.25 h / 25 °C

With copper(l) iodide; sodium azide; 2-propane phosphonic acid anhydride; potassium carbonate; triethylamine; trifluoroacetic acid; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;

Reference yield:

: 28229-69-8
2-(3-bromophenyl)ethan-1-ol

: 1201640-56-3
N-cyclohexyl-N-(2,2-dimethoxyethyl)-3-(3-(1-ethyl-1H-1,2,3-triazol-4-yl)phenethoxy)propanamide

Guidance literature:: Multi-step reaction with 6 steps

1: N-benzyl-trimethylammonium hydroxide / methanol; toluene / 24 h

2: triethylamine / copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 0.08 h / 100 °C / Microwave irradiation

3: potassium carbonate / methanol; dichloromethane / 1 h / 25 °C / Inert atmosphere

4: copper(l) iodide; sodium azide / water; tert-butyl alcohol / 6 h / 70 °C / Microwave irradiation

5: trifluoroacetic acid / dichloromethane / 0.5 h / 25 °C

6: 2-propane phosphonic acid anhydride; triethylamine / tetrahydrofuran; acetonitrile / 0.25 h / 25 °C

With copper(l) iodide; sodium azide; 2-propane phosphonic acid anhydride; N-benzyl-trimethylammonium hydroxide; potassium carbonate; triethylamine; trifluoroacetic acid; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol;