C₃₂H₄₀N₈O₁₁

Base Information

Chemical Name:C₃₂H₄₀N₈O₁₁
CAS No.:1415917-91-7
Molecular Formula:C₃₂H₄₀N₈O₁₁
Molecular Weight:712.717
Hs Code.:

C<sub>32</sub>H<sub>40</sub>N<sub>8</sub>O<sub>11</sub>

Synonyms:C₃₂H₄₀N₈O₁₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₄₀N₈O₁₁

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Technology Process of C₃₂H₄₀N₈O₁₁

There total 12 articles about C₃₂H₄₀N₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1415917-82-6
C₃₃H₄₂N₈O₁₁

: 1415917-91-7
C₃₂H₄₀N₈O₁₁

Guidance literature:: With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1039/c2cc36566a

Reference yield:

: 14260-27-6
3-deoxy-3-iodo-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 1415917-91-7
C₃₂H₄₀N₈O₁₁

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium azide / N,N-dimethyl-formamide / 105 °C

2.1: palladium 10% on activated carbon

3.1: sodium hydrogencarbonate / water; methanol

4.1: water; acetic acid

5.1: sodium periodate / water; methanol

6.1: potassium carbonate / methanol

7.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol

8.1: hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 760.05 Torr

9.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C

9.2: 24 h / 20 °C / Inert atmosphere

10.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 1 h / 0 °C

With sodium periodate; sodium azide; copper(ll) sulfate pentahydrate; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; acetic acid; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1039/c2cc36566a

Reference yield:

: 3-amino-3-deoxy-1,2:5,6-di-O-isopropylidene-D-glucofuranose

: 1415917-91-7
C₃₂H₄₀N₈O₁₁

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydrogencarbonate / water; methanol

2.1: water; acetic acid

3.1: sodium periodate / water; methanol

4.1: potassium carbonate / methanol

5.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol

6.1: hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 760.05 Torr

7.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C

7.2: 24 h / 20 °C / Inert atmosphere

8.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 1 h / 0 °C

With sodium periodate; copper(ll) sulfate pentahydrate; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; acetic acid; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1039/c2cc36566a