Technology Process of C19H22BIN2O2
There total 4 articles about C19H22BIN2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H33BN2O2Si;
With
Iodine monochloride;
In
dichloromethane;
at -78 ℃;
for 18h;
Inert atmosphere;
With
2-methyl-but-2-ene;
In
dichloromethane;
at 20 ℃;
for 0.0833333h;
Inert atmosphere;
DOI:10.1246/cl.130136
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene / 1 h / Inert atmosphere; Dean-Stark; Reflux
2.1: carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); norbornene / toluene / 20 h / 135 °C / Inert atmosphere
3.1: Iodine monochloride / dichloromethane / 18 h / -78 °C / Inert atmosphere
3.2: 0.08 h / 20 °C / Inert atmosphere
With
carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); norbornene; Iodine monochloride;
In
dichloromethane; toluene;
DOI:10.1246/cl.130136
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); norbornene / toluene / 20 h / 135 °C / Inert atmosphere
2.1: Iodine monochloride / dichloromethane / 18 h / -78 °C / Inert atmosphere
2.2: 0.08 h / 20 °C / Inert atmosphere
With
carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); norbornene; Iodine monochloride;
In
dichloromethane; toluene;
DOI:10.1246/cl.130136