3-amino-4-nitroacetophenone thiosemicarbazone

Base Information

Chemical Name:3-amino-4-nitroacetophenone thiosemicarbazone
CAS No.:1456532-30-1
Molecular Formula:C₉H₁₁N₅O₂S
Molecular Weight:253.285
Hs Code.:

Synonyms:3-amino-4-nitroacetophenone thiosemicarbazone

Suppliers and Price of 3-amino-4-nitroacetophenone thiosemicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-amino-4-nitroacetophenone thiosemicarbazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-amino-4-nitroacetophenone thiosemicarbazone

There total 4 articles about 3-amino-4-nitroacetophenone thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7463-31-2
3-Acetamidoacetophenone

: 1456532-30-1
3-amino-4-nitroacetophenone thiosemicarbazone

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid / acetic anhydride / 0 - 10 °C

2: hydrogenchloride / 4 h / Reflux

3: acetic acid / ethanol / 24 h / 20 °C

With hydrogenchloride; nitric acid; acetic acid; In ethanol; acetic anhydride;
DOI:10.1016/j.ejmech.2013.04.022

Reference yield:

: 79127-41-6
1-(3-amino-4-nitrophenyl)ethan-1-one

: 79-19-6
thiosemicarbazide

: 1456532-30-1
3-amino-4-nitroacetophenone thiosemicarbazone

Guidance literature:: With acetic acid; In ethanol; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2013.04.022

Reference yield:

: 99-03-6
1-(3-aminophenyl)ethanone

: 1456532-30-1
3-amino-4-nitroacetophenone thiosemicarbazone

Guidance literature:: Multi-step reaction with 4 steps

1: 1 h / 30 °C

2: nitric acid / acetic anhydride / 0 - 10 °C

3: hydrogenchloride / 4 h / Reflux

4: acetic acid / ethanol / 24 h / 20 °C

With hydrogenchloride; nitric acid; acetic acid; In ethanol; acetic anhydride;
DOI:10.1016/j.ejmech.2013.04.022