(1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol

Base Information

Chemical Name:(1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol
CAS No.:1621255-87-5
Molecular Formula:C₂₈H₂₉F₉N₂O₄
Molecular Weight:628.535
Hs Code.:

Synonyms:(1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol

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Chemical Property of (1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol

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Technology Process of (1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol

There total 4 articles about (1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₂₇F₉N₂O₄

: 1621255-87-5
(1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol

Guidance literature:: With sodium cyanoborohydride; In dichloromethane;

Reference yield:

: 344-39-8
4-methoxy-1-nitro-2-(trifluoromethyl)benzene

: 1621255-87-5
(1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: N-iodo-succinimide; sulfuric acid

2: copper; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / dimethyl sulfoxide / 16 h / 80 °C

3: acetic acid / dichloromethane / 0.5 h / 20 °C

4: sodium cyanoborohydride / dichloromethane

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-iodo-succinimide; sulfuric acid; copper; sodium cyanoborohydride; acetic acid; In dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1621256-17-4
C₈H₅F₃INO₃

: 1621255-87-5
(1R,2S)-1-(3,5-bis(trifluoromethyl)phenyl)-2-((2-(2-methoxy-5-nitro-4-(trifluoromethyl)phenyl)-5,5-dimethylcyclohex-1-enyl)methylamino)propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: copper; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / dimethyl sulfoxide / 16 h / 80 °C

2: acetic acid / dichloromethane / 0.5 h / 20 °C

3: sodium cyanoborohydride / dichloromethane

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper; sodium cyanoborohydride; acetic acid; In dichloromethane; dimethyl sulfoxide;