1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene

Base Information

• Chemical Name: 1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene
• CAS No.: 222054-67-3
• Molecular Formula: C₁₇H₁₄N₂O₆
• Molecular Weight: 342.308

Synonyms:1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene

Chemical Property of 1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene

Chemical Property:

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Technology Process of 1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene

There total 3 articles about 1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

nitromethane (75-52-5) + 3-(4-formylphenoxy)-4-methoxybenzaldehyde (2748-98-3) → 1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene (222054-67-3)

Guidance literature:

With ammonium acetate; In acetic acid; for 3h; Heating;

DOI:10.1021/jo9825198

Reference yield:

isovanillin (621-59-0) → 1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene (222054-67-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / K₂CO₃, CuO / pyridine / 12 h / 115 °C

2: 89 percent / NH₄OAc / acetic acid / 3 h / Heating

With ammonium acetate; potassium carbonate; copper(II) oxide; In pyridine; acetic acid;

DOI:10.1021/jo9825198

Reference yield:

4-bromo-benzaldehyde (1122-91-4) → 1-Methoxy-4-((Z)-2-nitro-vinyl)-2-[4-((E)-2-nitro-vinyl)-phenoxy]-benzene (222054-67-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / K₂CO₃, CuO / pyridine / 12 h / 115 °C

2: 89 percent / NH₄OAc / acetic acid / 3 h / Heating

With ammonium acetate; potassium carbonate; copper(II) oxide; In pyridine; acetic acid;

DOI:10.1021/jo9825198

upstream raw materials:

nitromethane

3-(4-formylphenoxy)-4-methoxybenzaldehyde

isovanillin

4-bromo-benzaldehyde

Downstream raw materials:

2-{3-[4-(2-amino-ethyl)-phenoxy]-4-methoxy-phenyl}-ethylamine

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