4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide

Base Information

Chemical Name:4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide
CAS No.:276681-97-1
Molecular Formula:C₂₃H₃₁N₃O₅S
Molecular Weight:461.582
Hs Code.:

Synonyms:4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide

Suppliers and Price of 4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide

There total 1 articles about 4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 57294-38-9
N-(tert-butoxycarbonyl)-4-aminobutanoic acid

: 244013-66-9
3-amino-N-(2,3-dimethylphenylbenzene sulphonamide)

: 276681-97-1
4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In N,N-dimethyl-formamide; at -15 - 20 ℃;
DOI:10.1211/146080800128735746

Reference yield:

: 276681-97-1
4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide

: 4-amino-N-[3-(2,3-dimethyl-phenylsulfamoyl)-phenyl]-butyramide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;
DOI:10.1211/146080800128735746

Reference yield:

: 276681-97-1
4-(tert-butyloxycarbonylamino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]butyric acid amide

: N-{3-[3-(2,3-dimethylphenylaminosulphonyl)phenylaminocarbonyl]propyl}pentadecanoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: HCl (gas) / dioxane / 2 h / 20 °C

2: 31 percent / N-methylmorpholine; isobutyl chloroformate / dimethylformamide / -15 - 20 °C

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1211/146080800128735746