2-phenylisocephalotaxine

Base Information

• Chemical Name: 2-phenylisocephalotaxine
• CAS No.: 73116-23-1
• Molecular Formula: C₂₄H₂₅NO₄
• Molecular Weight: 391.467

Synonyms:2-phenylisocephalotaxine

Chemical Property of 2-phenylisocephalotaxine

Chemical Property:

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Technology Process of 2-phenylisocephalotaxine

There total 1 articles about 2-phenylisocephalotaxine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

phenyllithium (591-51-5) + isocephalotaxinone (56144-23-1) → 2-phenylisocephalotaxine (73116-23-1)

Guidance literature:

In diethyl ether; for 7h; Ambient temperature;

DOI:10.1021/ja00523a029

Reference yield: 34.0%

2-phenylisocephalotaxine (73116-23-1) → benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; for 3h; Heating; oxidation;

DOI:10.1021/ja00523a029

upstream raw materials:

phenyllithium

isocephalotaxinone

Downstream raw materials:

benzoic acid

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