5-Hydroxy-9-methyl-2,2-diphenyl-7-trimethylsilanyloxy-6a,7,10,10a-tetrahydro-1,3-dioxa-cyclopenta[a]anthracene-6,11-dione

Base Information

Chemical Name:5-Hydroxy-9-methyl-2,2-diphenyl-7-trimethylsilanyloxy-6a,7,10,10a-tetrahydro-1,3-dioxa-cyclopenta[a]anthracene-6,11-dione
CAS No.:97485-97-7
Molecular Formula:C₃₁H₃₀O₆Si
Molecular Weight:526.661
Hs Code.:

Synonyms:5-Hydroxy-9-methyl-2,2-diphenyl-7-trimethylsilanyloxy-6a,7,10,10a-tetrahydro-1,3-dioxa-cyclopenta[a]anthracene-6,11-dione

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Chemical Property of 5-Hydroxy-9-methyl-2,2-diphenyl-7-trimethylsilanyloxy-6a,7,10,10a-tetrahydro-1,3-dioxa-cyclopenta[a]anthracene-6,11-dione

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Technology Process of 5-Hydroxy-9-methyl-2,2-diphenyl-7-trimethylsilanyloxy-6a,7,10,10a-tetrahydro-1,3-dioxa-cyclopenta[a]anthracene-6,11-dione

There total 4 articles about 5-Hydroxy-9-methyl-2,2-diphenyl-7-trimethylsilanyloxy-6a,7,10,10a-tetrahydro-1,3-dioxa-cyclopenta[a]anthracene-6,11-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 58274-64-9,82223-93-6,73912-36-4
(E)-trimethyl((3-methylbuta-1,3-dien-1-yl)oxy)silane

: 97467-30-6
5-hydroxy-2,2-diphenylnaphtho<1,2-d>-1,3-dioxole-6,9-dione

: 97485-97-7,102419-30-7,139341-77-8
(1RS,4aRS,9aRS)-5,6,8-trihydroxy-3-methyl-1-trimethylsilyloxy-1,4,4a,9a-tetrahydro-9,10-anthraquinone 5,6-benzophenone acetal

Guidance literature:: With tetraacetyl diborate; In diethyl ether; for 1h; Ambient temperature;

Reference yield:

: 2051-90-3
Dichlorodiphenylmethane

: 97485-97-7
5-Hydroxy-9-methyl-2,2-diphenyl-7-trimethylsilanyloxy-6a,7,10,10a-tetrahydro-1,3-dioxa-cyclopenta[a]anthracene-6,11-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / K₂CO₃*1.5 H₂O / acetonitrile / 20 h / Ambient temperature

2: tetraacetyldiborate / diethyl ether / 1 h / Ambient temperature

With tetraacetyl diborate; potassium carbonate; In diethyl ether; acetonitrile;
DOI:10.1021/jo00220a001

Reference yield:

: 13379-22-1
2,5,8-trihydroxy-1,4-naphthoquinone

: 97485-97-7
5-Hydroxy-9-methyl-2,2-diphenyl-7-trimethylsilanyloxy-6a,7,10,10a-tetrahydro-1,3-dioxa-cyclopenta[a]anthracene-6,11-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / K₂CO₃*1.5 H₂O / acetonitrile / 20 h / Ambient temperature

2: tetraacetyldiborate / diethyl ether / 1 h / Ambient temperature

With tetraacetyl diborate; potassium carbonate; In diethyl ether; acetonitrile;
DOI:10.1021/jo00220a001