5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione

Base Information

Chemical Name:5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione
CAS No.:852631-28-8
Molecular Formula:C₁₆H₁₀Br₂N₂O₃S
Molecular Weight:470.141
Hs Code.:

Synonyms:5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione

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Chemical Property of 5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione

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Technology Process of 5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione

There total 8 articles about 5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 852631-23-3
5-(4-(4-bromophenoxy)phenyl)-2-thioxodihydropyrimidine-4,6-dione

: 852631-28-8
5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 3h; Heating;
DOI:10.1021/jm049145x

Reference yield:

: 852631-08-4
[4-(4-bromophenoxy)phenyl]acetic acid

: 852631-28-8
5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / SOCl₂ / 1 h / Heating

2: 83 percent / NaH / dioxane / 3 h / Heating

3: 37 percent / EtONa / ethanol / 6 h / Heating

4: 36 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl₄ / 3 h / Heating

With N-Bromosuccinimide; thionyl chloride; sodium ethanolate; sodium hydride; dibenzoyl peroxide; In 1,4-dioxane; tetrachloromethane; ethanol;
DOI:10.1021/jm049145x

Reference yield:

: 852631-10-8
[4-(4-bromophenoxy)phenyl]acetic acid methyl ester

: 852631-28-8
5-bromo-5-[4-(4-bromophenoxy)phenyl]-2-thioxodihydropyrimidine-4,6-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaH / dioxane / 3 h / Heating

2: 37 percent / EtONa / ethanol / 6 h / Heating

3: 36 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl₄ / 3 h / Heating

With N-Bromosuccinimide; sodium ethanolate; sodium hydride; dibenzoyl peroxide; In 1,4-dioxane; tetrachloromethane; ethanol;
DOI:10.1021/jm049145x