(3aR,6aS)-1-Benzyl-2-trichloromethyl-3a,4,6,6a-tetrahydro-1H-thieno[3,4-d]imidazole 5,5-dioxide

Base Information

Chemical Name:(3aR,6aS)-1-Benzyl-2-trichloromethyl-3a,4,6,6a-tetrahydro-1H-thieno[3,4-d]imidazole 5,5-dioxide
CAS No.:87605-41-2
Molecular Formula:C₁₃H₁₃Cl₃N₂O₂S
Molecular Weight:367.683
Hs Code.:

Synonyms:(3aR,6aS)-1-Benzyl-2-trichloromethyl-3a,4,6,6a-tetrahydro-1H-thieno[3,4-d]imidazole 5,5-dioxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR,6aS)-1-Benzyl-2-trichloromethyl-3a,4,6,6a-tetrahydro-1H-thieno[3,4-d]imidazole 5,5-dioxide

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Technology Process of (3aR,6aS)-1-Benzyl-2-trichloromethyl-3a,4,6,6a-tetrahydro-1H-thieno[3,4-d]imidazole 5,5-dioxide

There total 2 articles about (3aR,6aS)-1-Benzyl-2-trichloromethyl-3a,4,6,6a-tetrahydro-1H-thieno[3,4-d]imidazole 5,5-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 87605-40-1
N-Benzyl-2,2,2-trichloro-N'-((3S,4R)-4-chloro-1,1-dioxo-tetrahydro-1λ⁶-thiophen-3-yl)-acetamidine

: 87605-41-2
(3aR,6aS)-1-Benzyl-2-trichloromethyl-3a,4,6,6a-tetrahydro-1H-thieno[3,4-d]imidazole 5,5-dioxide

Guidance literature:: With aluminum oxide; In acetonitrile; for 2h; Ambient temperature;
DOI:10.1246/cl.1983.1275

Reference yield:

: 87605-39-8
2,2,2-Trichloro-N-((3R,4S)-4-chloro-1,1-dioxo-tetrahydro-1λ⁶-thiophen-3-yl)-acetimidoyl chloride

: 87605-41-2
(3aR,6aS)-1-Benzyl-2-trichloromethyl-3a,4,6,6a-tetrahydro-1H-thieno[3,4-d]imidazole 5,5-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / triethylamine / tetrahydrofuran / 2.5 h / Ambient temperature

2: 85 percent / basic alumina / acetonitrile / 2 h / Ambient temperature

With aluminum oxide; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1246/cl.1983.1275