4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline

Base Information

Chemical Name:4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline
CAS No.:1255517-97-5
Molecular Formula:C₄₀H₃₂N₄S
Molecular Weight:600.787
Hs Code.:

Synonyms:4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline

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Chemical Property of 4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline

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Technology Process of 4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline

There total 5 articles about 4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 327061-54-1
9-bromo-6-butyl-6H-indolo[2,3-b]quinoxaline

: N,N-diphenyl-4-(5-(tributylbutylstannyl)thiophen-2-yl)aniline

: 1255517-97-5
4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 70 ℃; for 17h;
DOI:10.1021/jo1016663

Reference yield:

: 332929-55-2
5-bromo-1-butylindoline-2,3-dione

: 1255517-97-5
4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 17 h / 70 °C

With bis-triphenylphosphine-palladium(II) chloride; acetic acid; In N,N-dimethyl-formamide; 2: Stille coupling;
DOI:10.1021/jo1016663

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1255517-97-5
4-(5-(6-butyl-6H-indolo[2,3-b]quinoxalin-9-yl)thiophen-2-yl)-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 17 h / 70 °C

With bis-triphenylphosphine-palladium(II) chloride; acetic acid; In N,N-dimethyl-formamide; 2: Stille coupling;
DOI:10.1021/jo1016663