2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose

Base Information

Chemical Name:2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose
CAS No.:1412898-35-1
Molecular Formula:C₁₅H₁₅N₃O₅S
Molecular Weight:349.367
Hs Code.:

Synonyms:2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose

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Chemical Property of 2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose

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Technology Process of 2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose

There total 1 articles about 2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1412898-34-0
methyl 6-S-acetyl-3-azido-4-O-benzoyl-3-deoxy-6-thio-α-D-altropyranoside

: 108-24-7
acetic anhydride

: 1412898-35-1
2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose

Guidance literature:: With sulfuric acid; acetic acid; at 20 ℃;
DOI:10.1039/c2ob26308d

Reference yield: 83.0%

: 1412898-35-1
2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose

: 1412898-36-2
3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose

Guidance literature:: With water; guanidine nitrate; In ethanol; at 20 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1039/c2ob26308d

Reference yield:

: 1412898-35-1
2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose

: 1412898-37-3
3-azido-4-O-benzoyl-1,3-dideoxy-2-O-diazoacetyl-1-thio-1,6-anhydro-D-altropyranose

Guidance literature:: 2-O-acetyl-3-azido-4-O-benzoyl-1,3-dideoxy-1-thio-1,6-anhydro-D-altropyranose; With 2,2-dimethyl-5-(trifluoroacetyl)-1,3-dioxan-4,6-dione; In toluene; at 20 ℃; for 3h; Reflux; Inert atmosphere;

With p-carboxybenzenesulfonyl azide; triethylamine; In acetonitrile; at 0 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c2ob26308d