(E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene

Base Information

Chemical Name:(E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene
CAS No.:1379597-75-7
Molecular Formula:C₂₆H₂₁FO₆
Molecular Weight:450.426
Hs Code.:

(E,E)-1-fluoro-2,5-bis(3-methoxy[<sup>(13)</sup>C]carbonyl-4-hydroxystyryl)benzene

Synonyms:(E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene

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Technology Process of (E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene

There total 5 articles about (E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄⁽¹³⁾C₂H₁₉B₂Br₄FO₆

: 1379597-75-7
(E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene

Guidance literature:: With water; In hexane; dichloromethane; at 0 ℃;
DOI:10.1021/jo300746x

Reference yield:

: 1379597-73-5
(E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-methoxystyryl)benzene

: 1379597-75-7
(E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: boron tribromide / hexane; dichloromethane / -78 - 20 °C / Inert atmosphere

2: water / hexane; dichloromethane / 0 °C

With water; boron tribromide; In hexane; dichloromethane;
DOI:10.1021/jo300746x

Reference yield:

: 1379597-71-3
(E,E)-1-fluoro-2,5-bis(3-chloro-4-methoxystyryl)benzene

: 1379597-75-7
(E,E)-1-fluoro-2,5-bis(3-methoxy[⁽¹³⁾C]carbonyl-4-hydroxystyryl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 1,3-bis(dicyclohexylphosphino)propane bis(tetrafluoroborate) salt; palladium diacetate; potassium carbonate / dimethyl sulfoxide / 20 h / 120 °C / Molecular sieve

2: boron tribromide / hexane; dichloromethane / -78 - 20 °C / Inert atmosphere

3: water / hexane; dichloromethane / 0 °C

With 1,3-bis(dicyclohexylphosphino)propane bis(tetrafluoroborate) salt; water; palladium diacetate; boron tribromide; potassium carbonate; In hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jo300746x