4-(1-hydroxyethyl)-3-nitro-N-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethyl}benzamide

Base Information

• Chemical Name: 4-(1-hydroxyethyl)-3-nitro-N-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethyl}benzamide
• CAS No.: 1039151-82-0
• Molecular Formula: C₂₉H₃₈N₄O₁₀
• Molecular Weight: 602.642

Synonyms:4-(1-hydroxyethyl)-3-nitro-N-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethyl}benzamide

Chemical Property of 4-(1-hydroxyethyl)-3-nitro-N-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethyl}benzamide

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Technology Process of 4-(1-hydroxyethyl)-3-nitro-N-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethyl}benzamide

There total 1 articles about 4-(1-hydroxyethyl)-3-nitro-N-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethyl}benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

N-(2-{2-[2-(2-aminoethoxy)ethoxy]ethoxy}ethyl)-4-(1-hydroxyethyl)-3-nitrobenzamide (1039151-75-1) + 4-(4-oxopentanoylamino)benzoic acid (109098-54-6) → 4-(1-hydroxyethyl)-3-nitro-N-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethyl}benzamide (1039151-82-0)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

DOI:10.1021/jo800639p

Reference yield: 61.0%

4-(1-hydroxyethyl)-3-nitro-N-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethyl}benzamide (1039151-82-0) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → N,N-diisopropylphosphoramidous acid 2-cyanoethyl ester 1-(2-nitro-4-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethylcarbamoyl}phenyl)ethyl ester (1039151-85-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1.5h;

DOI:10.1021/jo800639p

upstream raw materials:

N-(2-{2-[2-(2-aminoethoxy)ethoxy]ethoxy}ethyl)-4-(1-hydroxyethyl)-3-nitrobenzamide

4-(4-oxopentanoylamino)benzoic acid

Downstream raw materials:

N,N-diisopropylphosphoramidous acid 2-cyanoethyl ester 1-(2-nitro-4-{2-[2-(2-{2-[4-(4-oxopentanoylamino)benzoylamino]ethoxy}ethoxy)ethoxy]ethylcarbamoyl}phenyl)ethyl ester

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