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C44H58N4O8

Base Information
  • Chemical Name:C44H58N4O8
  • CAS No.:1009094-30-7
  • Molecular Formula:C44H58N4O8
  • Molecular Weight:770.967
  • Hs Code.:
C<sub>44</sub>H<sub>58</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:C44H58N4O8

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Chemical Property of C44H58N4O8
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Technology Process of C44H58N4O8

There total 11 articles about C44H58N4O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tetrahydrofuran; at 20 ℃; for 1.5h;
Guidance literature:
Multi-step reaction with 2 steps
1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h
2: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran / 1.5 h / 20 °C
With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
Guidance literature:
Multi-step reaction with 8 steps
1.1: benzene / Heating / reflux
2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
2.2: 2 h
3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
4.2: 20 °C
4.3: 2 h
5.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.08 h
5.2: 1 h / 70 °C
6.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran / 0.83 h / 20 °C
7.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h
8.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran / 1.5 h / 20 °C
With titanium(IV) isopropylate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; trimethylaluminum; potassium acetate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; pyridine; hexane; dichloromethane; dimethyl sulfoxide; toluene; benzene;
upstream raw materials:

C44H58N4O7

C8H10INO2

C11H12INO4

C15H18INO5

Downstream raw materials:

C45H60N4O7

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