4',5'-dihydro-3'-phenylspiro

Base Information

Chemical Name:4',5'-dihydro-3'-phenylspiro
CAS No.:54848-13-4
Molecular Formula:C₁₂H₁₃NO
Molecular Weight:187.241
Hs Code.:

4',5'-dihydro-3'-phenylspiro<cyclobutane-1,5'-isoxazole>

Synonyms:4',5'-dihydro-3'-phenylspiro

Suppliers and Price of 4',5'-dihydro-3'-phenylspiro

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4',5'-dihydro-3'-phenylspiro

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4',5'-dihydro-3'-phenylspiro

There total 6 articles about 4',5'-dihydro-3'-phenylspiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1120-56-5
methylidenecyclobutane

: 698-16-8
benzohydroximoyl chloride

: 54848-13-4
4',5'-dihydro-3'-phenylspiro

Guidance literature:: With triethylamine; In diethyl ether; a) 0 deg C, 2 h, b) r.t., overnight;
DOI:10.1016/S0040-4020(01)89026-8

Reference yield: 81.0%

: (E)-4-nitrobenzaldehyde O-(1-(phenylethynyl)cyclobutyl)oxime

: 54848-13-4
4',5'-dihydro-3'-phenylspiro

Guidance literature:: With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); In methanol; at 50 ℃; for 24h; Inert atmosphere; Glovebox;
DOI:10.1055/s-0040-1707191

Reference yield:

: C₁₈H₁₂Co₂O₇

: 54848-13-4
4',5'-dihydro-3'-phenylspiro

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 2 h / -10 °C / Inert atmosphere; Glovebox

2: ammonium cerium (IV) nitrate / acetone / 2 h / 0 °C

3: [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I) / methanol / 24 h / 50 °C / Inert atmosphere; Glovebox

With ammonium cerium (IV) nitrate; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); boron trifluoride diethyl etherate; In methanol; dichloromethane; acetone; 1: |Nicholas Reaction;
DOI:10.1055/s-0040-1707191