S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolic acid hydrazide

Base Information

Chemical Name:S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolic acid hydrazide
CAS No.:837376-23-5
Molecular Formula:C₁₇H₁₄ClN₇OS
Molecular Weight:399.863
Hs Code.:

Synonyms:S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolic acid hydrazide

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Chemical Property of S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolic acid hydrazide

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Technology Process of S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolic acid hydrazide

There total 2 articles about S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 837376-21-3
ethyl-S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolate

: 837376-23-5
S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 4h; Heating;

Reference yield:

: 374088-63-8
6-(p-chlorophenyl)-7-phenyl-3-mercapto-1,2,4-triazolo-[4,3-b]-1,2,4-triazole

: 837376-23-5
S-[6-(p-chlorophenyl)-7-phenyl-1,2,4-triazolo[4,3-b]-1,2,4-triazole-3-yl]thioglycolic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / K₂CO₃ / acetone / 5 h / Heating

2: 76 percent / NH₂NH₂*H₂O / ethanol / 4 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; acetone;