Technology Process of 6-phenyl-2-(p-tolyl)phenanthridine
There total 5 articles about 6-phenyl-2-(p-tolyl)phenanthridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium tert-butylate; ethylene glycol;
In
toluene;
at 120 ℃;
for 18h;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/ol302489n
DOI:10.1021/ol302489n
- Guidance literature:
-
With
1,10-Phenanthroline; potassium tert-butylate;
In
toluene;
at 140 ℃;
for 20h;
Sealed tube;
DOI:10.1002/adsc.201900995
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; water / 12 h / 80 °C / Inert atmosphere
2: iodine; sodium hydrogencarbonate / water; dichloromethane / 20 °C
3: potassium tert-butylate; 1,10-Phenanthroline / toluene / 20 h / 140 °C / Sealed tube
With
bis-triphenylphosphine-palladium(II) chloride; 1,10-Phenanthroline; potassium tert-butylate; tetrabutyl ammonium fluoride; iodine; sodium hydrogencarbonate; potassium carbonate;
In
1,2-dimethoxyethane; dichloromethane; water; toluene;
DOI:10.1002/adsc.201900995
