2-cyanomethyl-N-(2-iodo-3,4-dimethoxybenzylidene)-4,5-(methylenedioxy)phenethylamine

Base Information

Chemical Name:2-cyanomethyl-N-(2-iodo-3,4-dimethoxybenzylidene)-4,5-(methylenedioxy)phenethylamine
CAS No.:1160948-98-0
Molecular Formula:C₂₀H₁₉IN₂O₄
Molecular Weight:478.286
Hs Code.:

Synonyms:2-cyanomethyl-N-(2-iodo-3,4-dimethoxybenzylidene)-4,5-(methylenedioxy)phenethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-cyanomethyl-N-(2-iodo-3,4-dimethoxybenzylidene)-4,5-(methylenedioxy)phenethylamine

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Technology Process of 2-cyanomethyl-N-(2-iodo-3,4-dimethoxybenzylidene)-4,5-(methylenedioxy)phenethylamine

There total 1 articles about 2-cyanomethyl-N-(2-iodo-3,4-dimethoxybenzylidene)-4,5-(methylenedioxy)phenethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 138490-95-6
2-iodo-3,4-dimethoxybenzaldehyde

: 1160948-77-5
N-[2-cyanomethyl-4,5-(methylenedioxy)phenethyl]trifluoroacetamide

: 1160948-98-0
2-cyanomethyl-N-(2-iodo-3,4-dimethoxybenzylidene)-4,5-(methylenedioxy)phenethylamine

Guidance literature:: With water; potassium carbonate; In methanol; at 20 ℃;
DOI:10.1021/jo900311g

Reference yield:

: 1160948-98-0
2-cyanomethyl-N-(2-iodo-3,4-dimethoxybenzylidene)-4,5-(methylenedioxy)phenethylamine

: 1-cyano-2-(2-iodo-3,4-dimethoxyphenyl)-7,8-(methylenedioxy)-1,2,4,5-tetrahydro-3H-3-benzazepine

Guidance literature:: With sodium t-butanolate; In tetrahydrofuran; tert-butyl alcohol; for 10h; Reflux; Inert atmosphere;
DOI:10.1021/jo900311g