C₅₉H₇₁N₃O₂₆

Base Information

Chemical Name:C₅₉H₇₁N₃O₂₆
CAS No.:213332-03-7
Molecular Formula:C₅₉H₇₁N₃O₂₆
Molecular Weight:1238.22
Hs Code.:

C<sub>59</sub>H<sub>71</sub>N<sub>3</sub>O<sub>26</sub>

Synonyms:C₅₉H₇₁N₃O₂₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₉H₇₁N₃O₂₆

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Technology Process of C₅₉H₇₁N₃O₂₆

There total 10 articles about C₅₉H₇₁N₃O₂₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 213331-80-7
C₆₂H₇₅N₃O₂₆

: 213332-03-7
C₅₉H₇₁N₃O₂₆

Guidance literature:: With acetic acid; at 20 - 40 ℃;
DOI:10.1021/ja980724z

Reference yield:

: 118358-66-0,73724-46-6
N-(9-fluorenylmethyloxycarbonyl)-L-serine benzyl ester

: 213332-03-7
C₅₉H₇₁N₃O₂₆

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / TMSOTf, 4A molecular sieves / tetrahydrofuran / 4 h / -78 °C

2: 100 percent / HOAc, TBAF / tetrahydrofuran / 72 h / Ambient temperature

3: BF₃*Et₂O, 4A molecular sieves / CH₂Cl₂ / a) -30 deg C, overnight, b) RT, 3 h

4: pyridine / Ambient temperature

5: 91 percent / 80percent aq. AcOH / 20 - 40 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja980724z

Reference yield:

: ((3aR,4R,7R,7aR)-7-Azido-2,2-dimethyl-6-nitrooxy-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethoxy)-triisopropyl-silane

: 213332-03-7
C₅₉H₇₁N₃O₂₆

Guidance literature:: Multi-step reaction with 7 steps

1: 99.8 percent / Et(i-Pr)2N, PhSH / acetonitrile / 1 h / 0 °C

2: 14 percent / K₂CO₃ / CH₂Cl₂ / 5 h / 0 - 20 °C

3: 66 percent / TMSOTf, 4A molecular sieves / tetrahydrofuran / 4 h / -78 °C

4: 100 percent / HOAc, TBAF / tetrahydrofuran / 72 h / Ambient temperature

5: BF₃*Et₂O, 4A molecular sieves / CH₂Cl₂ / a) -30 deg C, overnight, b) RT, 3 h

6: pyridine / Ambient temperature

7: 91 percent / 80percent aq. AcOH / 20 - 40 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; potassium carbonate; acetic acid; thiophenol; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ja980724z