2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide

Base Information

Chemical Name:2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide
CAS No.:1426585-11-6
Molecular Formula:C₂₄H₂₇N₂O₃P
Molecular Weight:422.464
Hs Code.:

Synonyms:2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide

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Chemical Property of 2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide

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Technology Process of 2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide

There total 3 articles about 2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1426585-16-1
2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine

: 1426585-11-6
2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide

Guidance literature:: With dihydrogen peroxide; acetic acid; In water; at 23 ℃; for 96h; Inert atmosphere;
DOI:10.1021/ic3025342

Reference yield:

: 4377-33-7
2-chloromethylpyridine

: 1426585-11-6
2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / toluene; hexane / 2 h / 80 - 90 °C / Inert atmosphere

1.2: 13 h / 23 - 90 °C / Inert atmosphere

2.1: dihydrogen peroxide; acetic acid / water / 96 h / 23 °C / Inert atmosphere

With n-butyllithium; dihydrogen peroxide; acetic acid; In hexane; water; toluene;
DOI:10.1021/ic3025342

Reference yield:

: 80413-42-9
oxide of diphenylphosphite

: 1426585-11-6
2-[(diphenyl-N,N-diethylcarbamoylmethylphosphine oxide)methyl]pyridine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / toluene; hexane / 2 h / 80 - 90 °C / Inert atmosphere

1.2: 13 h / 23 - 90 °C / Inert atmosphere

2.1: dihydrogen peroxide; acetic acid / water / 96 h / 23 °C / Inert atmosphere

With n-butyllithium; dihydrogen peroxide; acetic acid; In hexane; water; toluene;
DOI:10.1021/ic3025342