O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate

Base Information

Chemical Name:O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate
CAS No.:1353530-31-0
Molecular Formula:C₁₈H₁₇Cl₂NO₄S
Molecular Weight:414.309
Hs Code.:

Synonyms:O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate

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Chemical Property of O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate

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Technology Process of O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate

There total 4 articles about O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1353530-30-9
(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1-dioxolan-4-yl)methanol

: 1005-56-7
phenylcarbonochloridothioate

: 1353530-31-0
O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 213458-64-1
(2S)-2,3-O-isopropylidene-N,N-tetramethylenepropanamide

: 1353530-31-0
O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: TurboGrignard / tetrahydrofuran; cyclopentyl methyl ether / 0.25 h / -10 - -5 °C / Inert atmosphere

1.2: 0 - 20 °C

2.1: ethanol; sodium tetrahydroborate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; TurboGrignard; ethanol; In tetrahydrofuran; dichloromethane; cyclopentyl methyl ether;

Reference yield:

: 97966-00-2
5-bromo-2,3-dichloropyridine

: 1353530-31-0
O-(5,6-dichloropyridin-3-yl)((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl O-phenyl carbonothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: TurboGrignard / tetrahydrofuran; cyclopentyl methyl ether / 0.25 h / -10 - -5 °C / Inert atmosphere

1.2: 0 - 20 °C

2.1: ethanol; sodium tetrahydroborate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; TurboGrignard; ethanol; In tetrahydrofuran; dichloromethane; cyclopentyl methyl ether;