2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol

Base Information

Chemical Name:2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol
CAS No.:92982-69-9
Molecular Formula:C₄₅H₅₀Br₃ClO₁₃P₂
Molecular Weight:1136
Hs Code.:

Synonyms:2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol

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Chemical Property of 2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol

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Technology Process of 2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol

There total 11 articles about 2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.4%

: 92982-68-8
2-O-benzyl-3-O-(4-oxovaleryl)-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-chlorophenylphospho>-2,3-di-O-benzyl-sn-glycerol

: 92982-69-9
2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol

Guidance literature:: With pyridine; hydrazine hydrate; acetic acid; at 35 ℃; for 0.166667h;
DOI:10.1016/0008-6215(84)85277-5

Reference yield:

: 106401-57-4
1-O-allyl-2-O-benzyl-sn-glycerol

: 92982-69-9
2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol

Guidance literature:: Multi-step reaction with 7 steps

1: 86 percent / pyridine, 4-dimethylaminopyridine / dioxane / 3 h / 20 °C

2: 97 percent / 1,5-cyclooctadienebisiridinium hexafluorophosphate / various solvent(s) / 2 h / 20 °C

3: 91 percent / pyridine, acetic acid, hydrazine hydrate / 0.17 h / 35 °C

4: 1.) pyridine, 2.) 1-methylimidazole / 1.) oxolane, 20 deg C, 20 min, 2.) oxolane, 20 deg C, 2.5 h

5: 97 percent / mercuric oxide, mercuric chloride / acetone; H₂O / 0.75 h / 20 °C

6: 1.) 1-methylimidazole / 1.) oxolane, 20 deg C, 30 min, 2.) oxolane, 1.5 h, 20 deg C

7: 91.4 percent / pyridine, acetic acid, hydrazine hydrate / 0.17 h / 35 °C

With pyridine; 1-methyl-1H-imidazole; dmap; hydrazine hydrate; acetic acid; mercury dichloride; mercury(II) oxide; (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; In 1,4-dioxane; water; acetone;
DOI:10.1016/0008-6215(84)85277-5

Reference yield:

: 117606-89-0
1-O-trityl-2-O-benzyl-3-O-allyl-sn-glycerol

: 92982-69-9
2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol

Guidance literature:: Multi-step reaction with 8 steps

1: M hydrogen chloride / methanol; dioxane / 0.33 h

2: 86 percent / pyridine, 4-dimethylaminopyridine / dioxane / 3 h / 20 °C

3: 97 percent / 1,5-cyclooctadienebisiridinium hexafluorophosphate / various solvent(s) / 2 h / 20 °C

4: 91 percent / pyridine, acetic acid, hydrazine hydrate / 0.17 h / 35 °C

5: 1.) pyridine, 2.) 1-methylimidazole / 1.) oxolane, 20 deg C, 20 min, 2.) oxolane, 20 deg C, 2.5 h

6: 97 percent / mercuric oxide, mercuric chloride / acetone; H₂O / 0.75 h / 20 °C

7: 1.) 1-methylimidazole / 1.) oxolane, 20 deg C, 30 min, 2.) oxolane, 1.5 h, 20 deg C

8: 91.4 percent / pyridine, acetic acid, hydrazine hydrate / 0.17 h / 35 °C

With pyridine; 1-methyl-1H-imidazole; hydrogenchloride; dmap; hydrazine hydrate; acetic acid; mercury dichloride; mercury(II) oxide; (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; In 1,4-dioxane; methanol; water; acetone;
DOI:10.1016/0008-6215(84)85277-5