(2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine

Base Information

Chemical Name:(2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine
CAS No.:131105-38-9
Molecular Formula:C₄₁H₅₈F₃NO₁₃
Molecular Weight:829.906
Hs Code.:

Synonyms:(2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine

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Chemical Property of (2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine

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Technology Process of (2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine

There total 4 articles about (2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 18459-13-7
(2S,3R,4E)-3-O-benzoyl-N-trifluoroacetyl-4-sphingenine

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 131105-38-9
(2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine

Guidance literature:: With mercury(II) cyanide; In nitromethane; benzene; at 80 ℃; for 4h;

Reference yield:

: 130967-71-4
N-[(2S,3R,E)-1,3-dihydroxyoctadec-4-en-2-yl]-2,2,2-trifluoroacetamide

: 131105-38-9
(2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / pyridine / 14 h / 45 °C

2: 93 percent / pyridine / 18 h / Ambient temperature

3: 89 percent / Amberlyst 15 / CHCl₃; methanol / 40 h / Ambient temperature

4: 71 percent / mercuric cyanide / benzene; nitromethane / 4 h / 80 °C

With pyridine; Amberlyst 15; mercury(II) cyanide; In methanol; nitromethane; chloroform; benzene;

Reference yield:

: 131105-36-7
(2S,3R,4E)-N-trifluoroacetyl-1-O-trityl-4-sphingenine

: 131105-38-9
(2S,3R,4E)-3-O-benzoyl-1-O-(tetra-O-acetyl-β-D-glucopyranosyl)-N-trifluoroacetyl-4-sphingenine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine / 18 h / Ambient temperature

2: 89 percent / Amberlyst 15 / CHCl₃; methanol / 40 h / Ambient temperature

3: 71 percent / mercuric cyanide / benzene; nitromethane / 4 h / 80 °C

With pyridine; Amberlyst 15; mercury(II) cyanide; In methanol; nitromethane; chloroform; benzene;