methyl 11-({(2R,S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanoyl}amino)undecanoate

Base Information

Chemical Name:methyl 11-({(2R,S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanoyl}amino)undecanoate
CAS No.:805230-93-7
Molecular Formula:C₂₆H₄₂N₂O₅
Molecular Weight:462.63
Hs Code.:

Synonyms:methyl 11-({(2R,S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanoyl}amino)undecanoate

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Chemical Property of methyl 11-({(2R,S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanoyl}amino)undecanoate

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Technology Process of methyl 11-({(2R,S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanoyl}amino)undecanoate

There total 2 articles about methyl 11-({(2R,S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanoyl}amino)undecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4530-18-1
2-(tert-butoxycarbonylamino)-3-phenylpropionic acid

: 29833-32-7
11-aminoundecanoic acid methyl ester hydrochloride

: 805230-93-7
methyl 11-({(2R,S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanoyl}amino)undecanoate

Guidance literature:: With dmap; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1002/ejoc.200400105

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 805230-93-7
methyl 11-({(2R,S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanoyl}amino)undecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaOH; NaHCO₃ / dioxane; H₂O / 20 °C

2: 91 percent / DCC; DMAP; Et₃N / CH₂Cl₂ / 20 °C

With dmap; sodium hydroxide; sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1002/ejoc.200400105