(S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide

Base Information

• Chemical Name: (S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide
• CAS No.: 1232168-39-6
• Molecular Formula: C₁₈H₂₆N₂O₄S
• Molecular Weight: 366.481

Synonyms:(S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide

Chemical Property of (S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide

Chemical Property:

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Technology Process of (S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide

There total 1 articles about (S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H24N2O4S (1232168-38-5) + propargyl bromide (106-96-7) → (S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide (1232168-39-6)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 24h;

DOI:10.1021/ol101034s

Reference yield: 95.0%

(S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide (1232168-39-6) → (S)-2-(N-(3-chloroprop-2-ynyl)-4-methylphenylsulfonamido)-Nmethoxy-N,4-dimethylpentanamide

Guidance literature:

With N-chloro-succinimide; silver(I) acetate; In acetone; for 2.5h; Inert atmosphere; Reflux;

DOI:10.1021/acs.joc.8b01440

Reference yield:

(S)-2-(N-(prop-2-ynyl)-4-methylphenylsulfonamido)-N-methoxy-N,4-dimethylpentanamide (1232168-39-6) → C16H21NO3S (1232168-40-9)

Guidance literature:

With diisobutylaluminium hydride; In hexane; dichloromethane;

DOI:10.1021/ol101034s

upstream raw materials:

C₁₅H₂₄N₂O₄S

propargyl bromide

Downstream raw materials:

C₁₆H₂₁NO₃S

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