diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate

Base Information

Chemical Name:diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate
CAS No.:1364685-26-6
Molecular Formula:C₁₇H₂₇BO₅
Molecular Weight:322.209
Hs Code.:

Synonyms:diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate

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Chemical Property of diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate

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Technology Process of diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate

There total 4 articles about diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 5419-55-6
Triisopropyl borate

: 1364685-20-0
2-(2-bromo-3-ethoxyphenyl)-1,3-dioxolane

: 1364685-26-6
diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate

Guidance literature:: 2-(2-bromo-3-ethoxyphenyl)-1,3-dioxolane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;

Triisopropyl borate; In tetrahydrofuran; at -78 ℃; for 4h;

Reference yield:

: 196081-71-7
2-bromo-3-hydroxy-benzaldehyde

: 1364685-26-6
diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 70 °C

2.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

3.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

3.2: 4 h / -78 °C

With n-butyllithium; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1221180-39-7
2-bromo-3-ethoxybenzaldehyde

: 1364685-26-6
diisopropyl 2-(1,3-dioxolan-2-yl)-6-ethoxyphenylboronate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

2.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

2.2: 4 h / -78 °C

With n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;