1',2',3'-Trideoxy-4'-O-benzoyl-3'-(N-6-benzoyl-9-adenyl)-D-threo-pent-1'-enopyranose

Base Information

Chemical Name:1',2',3'-Trideoxy-4'-O-benzoyl-3'-(N-6-benzoyl-9-adenyl)-D-threo-pent-1'-enopyranose
CAS No.:139212-62-7
Molecular Formula:C₂₄H₁₉N₅O₄
Molecular Weight:441.446
Hs Code.:

Synonyms:1',2',3'-Trideoxy-4'-O-benzoyl-3'-(N-6-benzoyl-9-adenyl)-D-threo-pent-1'-enopyranose

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Chemical Property of 1',2',3'-Trideoxy-4'-O-benzoyl-3'-(N-6-benzoyl-9-adenyl)-D-threo-pent-1'-enopyranose

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Technology Process of 1',2',3'-Trideoxy-4'-O-benzoyl-3'-(N-6-benzoyl-9-adenyl)-D-threo-pent-1'-enopyranose

There total 3 articles about 1',2',3'-Trideoxy-4'-O-benzoyl-3'-(N-6-benzoyl-9-adenyl)-D-threo-pent-1'-enopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13475-85-9
1,3,4-Tri-O-benzoyl-2-deoxy-α,β-D-ribopyranose

: 139212-62-7,139342-69-1
Benzoic acid (S)-4-(6-benzoylamino-purin-9-yl)-3,4-dihydro-2H-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / HCl / CH₂Cl₂ / 1 h / 0 °C

2: 1) silylation, 2) CH₂Cl₂, molecular sieves 4 Angstroem, reflux, 3 h

With hydrogenchloride; In dichloromethane;
DOI:10.1016/S0040-4020(01)96048-X

Reference yield:

: 13475-85-9
1,3,4-Tri-O-benzoyl-2-deoxy-α,β-D-ribopyranose

: 4005-49-6
N₆-benzoyladenine

: 139212-62-7
1',2',3'-Trideoxy-4'-O-benzoyl-3'-(N-6-benzoyl-9-adenyl)-D-threo-pent-1'-enopyranose

: 1',2',3'-Trideoxy-4'-O-benzoyl-3'-(N-6-benzoyl-9-adenyl)-D-erythro-pent-1'-enopyranose

: 138373-38-3
N-6-Benzoyl-9-(2'-deoxy-3',4'-di-O-benzoyl-β-D-ribopyranosyl)adenine

Guidance literature:: With titanium tetrachloride; Yield given. Multistep reaction. Yields of byproduct given; 1) silylation, 2a) 1,2-dichloroethane, reflux, 4 h, 2b) r.t., overnight;
DOI:10.1016/S0040-4020(01)96048-X

Reference yield:

: 4005-49-6
N₆-benzoyladenine

: 99808-43-2
1-Chloro-3,4-di-O-benzoyl-2-deoxy-α,β-D-ribopyranose

: 139212-62-7,139342-69-1
Benzoic acid (S)-4-(6-benzoylamino-purin-9-yl)-3,4-dihydro-2H-pyran-3-yl ester

Guidance literature:: Yield given. Multistep reaction; 1) silylation, 2) CH₂Cl₂, molecular sieves 4 Angstroem, reflux, 3 h;
DOI:10.1016/S0040-4020(01)96048-X