1-(4-chlorophenyl)-4-hydroxy-3-phenyl-6-(2-thienyl)-2(1H)-pyridinone

Base Information

Chemical Name:1-(4-chlorophenyl)-4-hydroxy-3-phenyl-6-(2-thienyl)-2(1H)-pyridinone
CAS No.:230637-99-7
Molecular Formula:C₂₁H₁₄ClNO₂S
Molecular Weight:379.867
Hs Code.:
Mol file:230637-99-7.mol

Synonyms:1-(4-chloro-phenyl)-4-hydroxy-3-phenyl-6-thiophen-2-yl-1H-pyridin-2-one

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Chemical Property of 1-(4-chlorophenyl)-4-hydroxy-3-phenyl-6-(2-thienyl)-2(1H)-pyridinone

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Technology Process of 1-(4-chlorophenyl)-4-hydroxy-3-phenyl-6-(2-thienyl)-2(1H)-pyridinone

There total 4 articles about 1-(4-chlorophenyl)-4-hydroxy-3-phenyl-6-(2-thienyl)-2(1H)-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 83-13-6
diethyl 2-phenylmalonate

: 230637-90-8
(4-Chloro-phenyl)-[1-thiophen-2-yl-eth-(Z)-ylidene]-amine

: 230637-99-7
1-(4-chloro-phenyl)-4-hydroxy-3-phenyl-6-thiophen-2-yl-1H-pyridin-2-one

Guidance literature:: In diphenylether; at 250 ℃; for 2h;
DOI:10.1002/jhet.5570360234

Reference yield:

: 88-15-3,97511-16-5
2-Acetylthiophene

: 230637-99-7
1-(4-chloro-phenyl)-4-hydroxy-3-phenyl-6-thiophen-2-yl-1H-pyridin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / glacial acetic acid / a) 0 deg C, 4-5 h, b) RT, overnight

2: 94 percent / KOH / methanol / 1 h / Heating

3: 50 percent / diphenyl ether / 2 h / 250 °C

With potassium hydroxide; acetic acid; In methanol; diphenylether;
DOI:10.1002/jhet.5570360234

Reference yield:

: 106-47-8
4-chloro-aniline

: 230637-99-7
1-(4-chloro-phenyl)-4-hydroxy-3-phenyl-6-thiophen-2-yl-1H-pyridin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / glacial acetic acid / a) 0 deg C, 4-5 h, b) RT, overnight

2: 94 percent / KOH / methanol / 1 h / Heating

3: 50 percent / diphenyl ether / 2 h / 250 °C

With potassium hydroxide; acetic acid; In methanol; diphenylether;
DOI:10.1002/jhet.5570360234