4-(2-(tert-butyldimethylsilyloxy)ethyl)-N-(3,3-diphenylpropyl)benzenamine

Base Information

• Chemical Name: 4-(2-(tert-butyldimethylsilyloxy)ethyl)-N-(3,3-diphenylpropyl)benzenamine
• CAS No.: 1101174-11-1
• Molecular Formula: C₂₉H₃₉NOSi
• Molecular Weight: 445.72

Synonyms:4-(2-(tert-butyldimethylsilyloxy)ethyl)-N-(3,3-diphenylpropyl)benzenamine

Chemical Property of 4-(2-(tert-butyldimethylsilyloxy)ethyl)-N-(3,3-diphenylpropyl)benzenamine

Chemical Property:

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Technology Process of 4-(2-(tert-butyldimethylsilyloxy)ethyl)-N-(3,3-diphenylpropyl)benzenamine

There total 1 articles about 4-(2-(tert-butyldimethylsilyloxy)ethyl)-N-(3,3-diphenylpropyl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-diphenylpropyl amine (5586-73-2) + 1-(t-butyldimethylsilyloxy)-2-(4-bromophenyl)ethane (73899-15-7) → 4-(2-(tert-butyldimethylsilyloxy)ethyl)-N-(3,3-diphenylpropyl)benzenamine (1101174-11-1)

Guidance literature:

With potassium phosphate; copper(l) iodide; L-proline; In dimethyl sulfoxide; at 90 ℃; for 24h;

Reference yield:

N-(4-(2-amino-5-chlorothiazol-4-yl)phenyl)-methanesulfonamide (1002566-71-3) + 4-(2-(tert-butyldimethylsilyloxy)ethyl)-N-(3,3-diphenylpropyl)benzenamine (1101174-11-1) + 1,1'-carbonyldiimidazole (530-62-1) → 1-(4-(2-(tert-butyldimethylsilyloxy)ethyl)phenyl)-3-(5-chloro-4-(4-(methylsulfonamido)phenyl)thiazol-2-yl)-1-(3,3-diphenylpropyl)urea (1101174-12-2)

Guidance literature:

With dmap; In N,N-dimethyl-formamide; at 40 ℃; for 48h;

upstream raw materials:

3-diphenylpropyl amine

1-(t-butyldimethylsilyloxy)-2-(4-bromophenyl)ethane

Downstream raw materials:

1-(4-(2-(tert-butyldimethylsilyloxy)ethyl)phenyl)-3-(5-chloro-4-(4-(methylsulfonamido)phenyl)thiazol-2-yl)-1-(3,3-diphenylpropyl)urea

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