2,5-DICHLOROANILINE-3,4,6-D3

Base Information

• Chemical Name: 2,5-DICHLOROANILINE-3,4,6-D3
• CAS No.: 783321-80-2
• Molecular Formula: C6H2 Cl2 D3 N
• Molecular Weight: 164.995
• Mol file: 783321-80-2.mol

Synonyms:2,5-DICHLOROANILINE-3,4,6-D3

Chemical Property of 2,5-DICHLOROANILINE-3,4,6-D3

Chemical Property:

• PSA: 26.02000
• LogP: 3.15680
• Storage Temp.: -20°C Freezer, Under inert atmosphere
• Solubility.: Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

2,5-DICHLOROANILINE-3,4,6-D3 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,5-Dichloroaniline-3,4,6-d3 (CAS# 783321-80-2) is a useful isotopically labeled research compound.

Technology Process of 2,5-DICHLOROANILINE-3,4,6-D3

There total 2 articles about 2,5-DICHLOROANILINE-3,4,6-D3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

[3,4,6-(2)H3]-2,5-dichloronitrobenzene (783321-79-9) → [3,4,6-(2)H3]-2,5-dichloroaniline (783321-80-2)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; atmospheric pressure;

DOI:10.1039/b409373a

Reference yield:

1,4-dichlorobenzene-d4 (3855-82-1) → [3,4,6-(2)H3]-2,5-dichloroaniline (783321-80-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / fuming nitric acid / 0.25 h / 20 °C

2: 84 percent / aq. HCl; hydrogen / Pd/C / methanol / 20 °C / atmospheric pressure

With hydrogenchloride; hydrogen; nitric acid; palladium on activated charcoal; In methanol;

DOI:10.1039/b409373a

upstream raw materials:

[3,4,6-⁽²⁾H₃]-2,5-dichloronitrobenzene

1,4-dichlorobenzene-d4

Refernces