[2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine

Base Information

Chemical Name:[2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine
CAS No.:188608-15-3
Molecular Formula:C₃₂H₄₁NP₂Si₂
Molecular Weight:557.803
Hs Code.:

Synonyms:[2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine

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Chemical Property of [2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine

Chemical Property:

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Technology Process of [2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine

There total 7 articles about [2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2155-96-6
Diphenylvinylphosphine

: 188608-12-0
[3-(1,1,1,3,3,3-Hexamethyl-disilazan-2-yl)-phenyl]-phenyl-phosphane

: 188608-15-3
[2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In toluene; at 70 ℃; for 96h;
DOI:10.1021/jo961140n

Reference yield:

: 4073-31-8
(diethylamino)phenylchlorophosphine

: 188608-15-3
[2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / tetrahydrofuran / 16 h / Ambient temperature

2: toluene / 12 h / Heating

3: 1.) LiAlH₄, 2.) Na / 1.) Et₂O, rt, 3 h, 2.) methyl tert-butyl ether, reflux, 28 h

4: 89 percent / AIBN / toluene / 96 h / 70 °C

With lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); sodium; In tetrahydrofuran; toluene;
DOI:10.1021/jo961140n

Reference yield:

: 188608-09-5
[3-(N,N-bis(trimethylsilyl)amino)phenyl](dimethylamino)phenylphosphine

: 188608-15-3
[2-(diphenylphosphino)ethyl][3-(N,N-bis(trimethylsilyl)amino)phenyl]phenylphosphine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 0.17 h / Heating

2: 1.) LiAlH₄, 2.) Na / 1.) Et₂O, rt, 3 h, 2.) methyl tert-butyl ether, reflux, 28 h

3: 89 percent / AIBN / toluene / 96 h / 70 °C

With lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); sodium; In toluene;
DOI:10.1021/jo961140n