N^α-benzyloxycarbonyl-N^δ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester

Base Information

• Chemical Name: N^α-benzyloxycarbonyl-N^δ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester
• CAS No.: 370579-56-9
• Molecular Formula: C₂₃H₂₉N₃O₈S
• Molecular Weight: 507.565

Synonyms:N^α-benzyloxycarbonyl-N^δ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester

Chemical Property of N^α-benzyloxycarbonyl-N^δ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester

Chemical Property:

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Technology Process of N^α-benzyloxycarbonyl-N^δ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester

There total 1 articles about N^α-benzyloxycarbonyl-N^δ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-Benzyloxycarbonylamino-5-(2-nitro-benzenesulfonylamino)-pentanoic acid → Nα-benzyloxycarbonyl-Nδ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester (370579-56-9)

Guidance literature:

DOI:10.1016/S0040-4039(01)01062-0

Reference yield: 96.0%

2,2-Dimethyl-propionic acid 3-((3aR,4R,6R,6aR)-6-hydroxymethyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester (370579-50-3) + Nα-benzyloxycarbonyl-Nδ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester (370579-56-9) → 2-benzyloxycarbonylamino-5-[{6-[3-(2,2-dimethyl-propionyloxymethyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl}-(2-nitro-benzenesulfonyl)-amino]-pentanoic acid tert-butyl ester

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at -50 - 20 ℃;

DOI:10.1016/S0040-4039(01)01062-0

Reference yield: 95.0%

methyl 2,3,4-tri-O-benzyl-D-glucopyranoside (53008-65-4,641635-63-4) + Nα-benzyloxycarbonyl-Nδ-(2-nitrobenzenesulfonyl)-L-ornithine tert-butyl ester (370579-56-9) → (S)-2-Benzyloxycarbonylamino-5-[(2-nitro-benzenesulfonyl)-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl)-amino]-pentanoic acid tert-butyl ester

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at -50 - 20 ℃;

DOI:10.1016/S0040-4039(01)01062-0

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