C₂₅H₃₇N

Base Information

Chemical Name:C₂₅H₃₇N
CAS No.:1380217-82-2
Molecular Formula:C₂₅H₃₇N
Molecular Weight:351.575
Hs Code.:

Synonyms:C₂₅H₃₇N

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Chemical Property of C₂₅H₃₇N

Chemical Property:

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Technology Process of C₂₅H₃₇N

There total 4 articles about C₂₅H₃₇N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14519-31-4
1-ethynylcyclododecan-1-ol

: 1380217-82-2
C₂₅H₃₇N

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 37.17 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1.42 h / -20 °C / Inert atmosphere

2.2: 19 h / -20 - 20 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / diethyl ether / 4.75 h / 0 °C / Inert atmosphere; Reflux

4.1: triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

5.1: triethylamine; sodium iodide / dimethyl sulfoxide / 5 h / 50 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; toluene-4-sulfonic acid; triethylamine; sodium iodide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/anie.201107747

Reference yield:

: 1-ethynyl-1-(tetrahydropyran-2-yloxy)-cyclododecane

: 1380217-82-2
C₂₅H₃₇N

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.42 h / -20 °C / Inert atmosphere

1.2: 19 h / -20 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 4.75 h / 0 °C / Inert atmosphere; Reflux

3.1: triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

4.1: triethylamine; sodium iodide / dimethyl sulfoxide / 5 h / 50 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; triethylamine; sodium iodide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/anie.201107747

Reference yield:

: C₂₀H₃₄O₃

: 1380217-82-2
C₂₅H₃₇N

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 4.75 h / 0 °C / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

3: triethylamine; sodium iodide / dimethyl sulfoxide / 5 h / 50 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; sodium iodide; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/anie.201107747