O-[(E)-4-(tert-butoxycarbonyl(phenyl)amino)but-2-enyl] dimethylthiocarbamate

Base Information

Chemical Name:O-[(E)-4-(tert-butoxycarbonyl(phenyl)amino)but-2-enyl] dimethylthiocarbamate
CAS No.:1018479-21-4
Molecular Formula:C₁₈H₂₆N₂O₃S
Molecular Weight:350.482
Hs Code.:

Synonyms:O-[(E)-4-(tert-butoxycarbonyl(phenyl)amino)but-2-enyl] dimethylthiocarbamate

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Chemical Property of O-[(E)-4-(tert-butoxycarbonyl(phenyl)amino)but-2-enyl] dimethylthiocarbamate

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Technology Process of O-[(E)-4-(tert-butoxycarbonyl(phenyl)amino)but-2-enyl] dimethylthiocarbamate

There total 1 articles about O-[(E)-4-(tert-butoxycarbonyl(phenyl)amino)but-2-enyl] dimethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1018479-39-4
tert-butyl (E)-(4-hydroxybut-2-en-1-yl)(phenyl)carbamate

: 16420-13-6
N,N-Dimethylthiocarbamoyl chloride

: 1018479-21-4
O-[(E)-4-(tert-butoxycarbonyl(phenyl)amino)but-2-enyl] dimethylthiocarbamate

Guidance literature:: tert-butyl (E)-(4-hydroxybut-2-en-1-yl)(phenyl)carbamate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

N,N-Dimethylthiocarbamoyl chloride; With sodium iodide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃;
DOI:10.1021/ol8002942

Reference yield:

: 1018479-21-4
O-[(E)-4-(tert-butoxycarbonyl(phenyl)amino)but-2-enyl] dimethylthiocarbamate

: S-[(S)-1-(tert-butoxycarbonyl(phenyl)amino)but-3-en-2-yl] dimethylthiocarbamate

: 1018479-32-7
S-[(R)-1-(tert-butoxycarbonyl(phenyl)amino)but-3-en-2-yl] dimethylthiocarbamate

Guidance literature:: With di-μ-chlorobis[(η5-(S)-(ρR)-2-(2'-(4'-methylethyl)oxazolinyl)cyclopentadienyl, 1-C,3'-N)(η4-tetraphenylcyclobutadiene)cobalt]dipalladium; In dichloromethane; at 40 ℃; for 43h; optical yield given as %ee;
DOI:10.1021/ol8002942