Benzenamine, 3-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)-4-methyl- (9CI)

Base Information

Chemical Name:Benzenamine, 3-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)-4-methyl- (9CI)
CAS No.:782499-18-7
Molecular Formula:C12H16 N2 O
Molecular Weight:204.272
Hs Code.:
Mol file:782499-18-7.mol

Synonyms:Benzenamine, 3-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)-4-methyl- (9CI)

Suppliers and Price of Benzenamine, 3-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)-4-methyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Benzenamine, 3-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)-4-methyl- (9CI)

Chemical Property:

PSA：47.61000
LogP:2.14940

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenamine, 3-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)-4-methyl- (9CI)

There total 2 articles about Benzenamine, 3-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)-4-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 942605-68-7
N-(2-hydroxy-1,1-dimethyl-ethyl)-2-methyl-5-nitro-benzamide

: 782499-18-7
2-[(3-amino-6-methyl)phenyl]-4,4-dimethyloxazoline

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CH₂Cl₂ / 0.5 h / 20 °C

2: 896 mg / aq. NH₄Cl; Fe / ethanol / 3 h / Heating

With thionyl chloride; iron; ammonium chloride; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2006.10.006

Reference yield:

: 1975-52-6
5-nitro-o-toluic acid

: 782499-18-7
2-[(3-amino-6-methyl)phenyl]-4,4-dimethyloxazoline

Guidance literature:: Multi-step reaction with 3 steps

1: HBTU; N,N-diisopropylethylamine / dimethylformamide / 14 h / 40 °C

2: SOCl₂ / CH₂Cl₂ / 0.5 h / 20 °C

3: 896 mg / aq. NH₄Cl; Fe / ethanol / 3 h / Heating

With thionyl chloride; iron; ammonium chloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.10.006

Reference yield: 36.0%

: 782499-18-7
2-[(3-amino-6-methyl)phenyl]-4,4-dimethyloxazoline

: 2-[(3-amino-2-iodo-6-methyl)phenyl]-4,4-dimethyloxazoline

: 782499-20-1
2-[(3-amino-4-iodo-6-methyl)phenyl]-4,4-dimethyloxazoline

Guidance literature:: With Iodine monochloride; calcium carbonate; In methanol; dichloromethane; water; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2006.10.006