C₄₈H₆₇NO₇

Base Information

Chemical Name:C₄₈H₆₇NO₇
CAS No.:1354747-52-6
Molecular Formula:C₄₈H₆₇NO₇
Molecular Weight:770.062
Hs Code.:

C<sub>48</sub>H<sub>67</sub>NO<sub>7</sub>

Synonyms:C₄₈H₆₇NO₇

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Chemical Property of C₄₈H₆₇NO₇

Chemical Property:

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Technology Process of C₄₈H₆₇NO₇

There total 23 articles about C₄₈H₆₇NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1354747-51-5
C₅₆H₇₅NO₉

: 1354747-52-6
C₄₈H₆₇NO₇

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; ethanol; water; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol2032448

Reference yield:

: 201279-58-5
1-deoxy-1-allyl-2,3,4,6-tetra-O-acetyl-D-galactopyranoside

: 1354747-52-6
C₄₈H₆₇NO₇

Guidance literature:: Multi-step reaction with 16 steps

1.1: methanol; sodium methylate / 1 h / 20 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone / dichloromethane / 0.08 h / 55 °C / Inert atmosphere; Molecular sieve

6.2: 48 h / 55 °C / Inert atmosphere; Molecular sieve

7.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

7.2: 20 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.75 h / -40 °C / Inert atmosphere; Molecular sieve

8.2: 24 h / -40 - -20 °C / Inert atmosphere

9.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 0.67 h / 20 °C / Inert atmosphere

10.1: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

11.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / Inert atmosphere; Reflux

12.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

13.1: water; potassium carbonate / methanol / 20 °C / Inert atmosphere

14.1: triethylamine; trifluoroacetic anhydride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

15.1: tributyltin methoxide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

16.1: sodium hydroxide / tetrahydrofuran; ethanol; water / 4 h / 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; methanol; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); L-(+)-diisopropyl tartrate; tetrabutyl ammonium fluoride; water; iodine; sodium methylate; tributyltin methoxide; sodium hydride; potassium carbonate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2-phenyl-1,4-benzoquinone; trifluoroacetic anhydride; sodium hydroxide; zinc; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene; 8.1: Sharpless epoxidation / 8.2: Sharpless epoxidation;
DOI:10.1021/ol2032448

Reference yield:

: 1354747-41-3
C₃₁H₃₆O₅

: 1354747-52-6
C₄₈H₆₇NO₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone / dichloromethane / 0.08 h / 55 °C / Inert atmosphere; Molecular sieve

1.2: 48 h / 55 °C / Inert atmosphere; Molecular sieve

2.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.75 h / -40 °C / Inert atmosphere; Molecular sieve

3.2: 24 h / -40 - -20 °C / Inert atmosphere

4.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 0.67 h / 20 °C / Inert atmosphere

5.1: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / Inert atmosphere; Reflux

7.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

8.1: water; potassium carbonate / methanol / 20 °C / Inert atmosphere

9.1: triethylamine; trifluoroacetic anhydride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

10.1: tributyltin methoxide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

11.1: sodium hydroxide / tetrahydrofuran; ethanol; water / 4 h / 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); L-(+)-diisopropyl tartrate; water; iodine; sodium methylate; tributyltin methoxide; potassium carbonate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2-phenyl-1,4-benzoquinone; trifluoroacetic anhydride; sodium hydroxide; zinc; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; benzene; 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation;
DOI:10.1021/ol2032448