Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester

Base Information

• Chemical Name: Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester
• CAS No.: 207981-74-6
• Molecular Formula: C₂₄H₃₉BrO₅
• Molecular Weight: 487.475

Synonyms:Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester

Chemical Property of Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester

There total 3 articles about Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

acetic anhydride (108-24-7) + (R)-1-(12-Bromo-dodecyloxy)-3-(4-methoxy-phenoxy)-propan-2-ol (207981-71-3) → Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester (207981-74-6)

Guidance literature:

With dmap; In pyridine;

DOI:10.1016/S0040-4039(98)00418-3

Reference yield:

1,12-dibromododecane (3344-70-5) → Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester (207981-74-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) di-n-butyltin oxide; 2.) CsF / 1.) MeOH; 2.) DMF, rt.

2: 90 percent / DMAP / pyridine

With dmap; di(n-butyl)tin oxide; cesium fluoride; In pyridine;

DOI:10.1016/S0040-4039(98)00418-3

Reference yield:

(R)-3-(p-methoxyphenoxy)-1,2-propanediol (17131-52-1,124933-35-3,131064-88-5,131064-87-4) → Acetic acid (R)-1-(12-bromo-dodecyloxymethyl)-2-(4-methoxy-phenoxy)-ethyl ester (207981-74-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) di-n-butyltin oxide; 2.) CsF / 1.) MeOH; 2.) DMF, rt.

2: 90 percent / DMAP / pyridine

With dmap; di(n-butyl)tin oxide; cesium fluoride; In pyridine;

DOI:10.1016/S0040-4039(98)00418-3

upstream raw materials:

acetic anhydride

(R)-1-(12-Bromo-dodecyloxy)-3-(4-methoxy-phenoxy)-propan-2-ol

1,12-dibromododecane

(R)-3-(p-methoxyphenoxy)-1,2-propanediol

Downstream raw materials:

Hexanoic acid (R)-2-{[(3aR,4S,5S,6R,7R,7aS)-5-benzyloxy-6,7-bis-(bis-benzyloxy-phosphoryloxy)-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-4-yloxy]-hydroxy-phosphoryloxy}-1-[12-(naphthalen-2-yloxy)-dodecyloxymethyl]-ethyl ester

C₇₅H₉₅O₁₈P₃

Hexanoic acid (R)-2-[((3aR,4S,5R,5aR,8aS,8bR)-5-benzyloxy-2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yloxy)-hydroxy-phosphoryloxy]-1-[12-(naphthalen-2-yloxy)-dodecyloxymethyl]-ethyl ester

C₅₀H₇₃O₁₂P

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