1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane⁽¹²⁾

Base Information

Chemical Name:1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane⁽¹²⁾
CAS No.:372969-92-1
Molecular Formula:C₁₁H₂₀B₁₀S₂
Molecular Weight:324.522
Hs Code.:

1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane<sup>(12)</sup>

Synonyms:1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane⁽¹²⁾

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Chemical Property of 1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane⁽¹²⁾

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Technology Process of 1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane⁽¹²⁾

There total 1 articles about 1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane⁽¹²⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 17702-41-9
nido-decaborane

: 372969-91-0
2-(3-ethynylphenyl)-4,5-dihydro-1,3-dithiole

: 372969-92-1
1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane⁽¹²⁾

Guidance literature:: In acetonitrile; B-compound in MeCN was stirred under Ar for 4 h, ligand in MeCN was added, boiled under reflux for 3 d; evapd., chromd. with CHCl3-hexane;
DOI:10.1039/b209534c

Reference yield: 97.0%

: 372969-92-1
1-[3-(4,5-dihydro-1,3-dithiol-2-yl)phenyl]-1,2-dicarbaclosododecaborane⁽¹²⁾

: 130611-25-5
3-(1,2-dicarbaclosododecaboran⁽¹²⁾-1-yl)benzaldehyde

Guidance literature:: With Hg(ClO₄)2*H₂O; In tetrahydrofuran; B-compound was stirred with Hg(ClO4)2*H2O in THF for 5 min; filtered, evapd., washed with aq. Na2CO3, water and brine, dried, evapd.;
DOI:10.1039/b209534c