2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole

Base Information

Chemical Name:2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole
CAS No.:132402-73-4
Molecular Formula:C₁₇H₁₈N₂O₄S
Molecular Weight:346.407
Hs Code.:

Synonyms:2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole

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Chemical Property of 2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole

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Technology Process of 2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole

There total 5 articles about 2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.6%

: 132402-65-4
2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonyl-(R)-Δ2-thiazoline

: 132402-73-4
2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole

Guidance literature:: With manganese(IV) oxide; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(01)81482-4

Reference yield:

: 90508-20-6
N-allyloxycarbonyl-(S)-phenylalanate

: 132402-73-4
2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / acetyl chloride / Ambient temperature

2: 99 percent / NH₃ / methanol / Ambient temperature

3: 97 percent / CH₂Cl₂ / Ambient temperature

4: 20 percent / ethanol / 2 h / Ambient temperature

5: 86.6 percent / activated MnO₂ / CH₂Cl₂ / Ambient temperature

With manganese(IV) oxide; ammonia; acetyl chloride; In methanol; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)81482-4

Reference yield:

: 132402-50-7
(S)-N-(allyloxycarbonyl)phenylalaninamide

: 132402-73-4
2-<(S)-1-allyloxycarbonylamino-2-phenyl-ethyl>-4-methoxycarbonylthiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / CH₂Cl₂ / Ambient temperature

2: 20 percent / ethanol / 2 h / Ambient temperature

3: 86.6 percent / activated MnO₂ / CH₂Cl₂ / Ambient temperature

With manganese(IV) oxide; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)81482-4