(2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester

Base Information

Chemical Name:(2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester
CAS No.:154061-65-1
Molecular Formula:C₁₅H₂₀BrNO₄
Molecular Weight:358.232
Hs Code.:

Synonyms:(2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester

Suppliers and Price of (2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester

There total 3 articles about (2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 154061-64-0
(2S)-2-<(Benzyloxycarbonyl)amino>-6-hydroxyhexanoic acid methyl ester

: 154061-65-1
(2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/jo00083a011

Reference yield:

: 2212-75-1
N₂-[(benzyloxy)carbonyl]-L-lysine

: 154061-65-1
(2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium nitroprusside dihydrate, aq. NaOH / 6 h / 60 °C

2: diethyl ether; ethyl acetate

3: 87 percent / CBr₄, triphenylphosphine / CH₂Cl₂ / 0.5 h / 0 °C

With sodium nitroprusside; sodium hydroxide; carbon tetrabromide; triphenylphosphine; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jo00083a011

Reference yield:

: 102922-72-5
(S)-2-(((benzyloxy)carbonyl)amino)-6-hydroxyhexanoic acid

: 154061-65-1
(2S)-2-<(Benzyloxycarbonyl)amino>-6-bromohexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; ethyl acetate

2: 87 percent / CBr₄, triphenylphosphine / CH₂Cl₂ / 0.5 h / 0 °C

With carbon tetrabromide; triphenylphosphine; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jo00083a011