3-ethyl 4-methyl 1-methoxy-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

Base Information

Chemical Name:3-ethyl 4-methyl 1-methoxy-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate
CAS No.:1257649-36-7
Molecular Formula:C₁₆H₁₆N₂O₇
Molecular Weight:348.312
Hs Code.:

Synonyms:3-ethyl 4-methyl 1-methoxy-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

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Chemical Property of 3-ethyl 4-methyl 1-methoxy-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

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Technology Process of 3-ethyl 4-methyl 1-methoxy-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

There total 2 articles about 3-ethyl 4-methyl 1-methoxy-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1257649-11-8
(Z)-ethyl 2-diazo-3-(methoxyimino)-3-(4-nitrophenyl)propanoate

: 999-59-7,20664-47-5
methyl (2E)-3-(dimethylamino)prop-2-enoate

: 1257649-36-7
3-ethyl 4-methyl 1-methoxy-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

Guidance literature:: (Z)-ethyl 2-diazo-3-(methoxyimino)-3-(4-nitrophenyl)propanoate; methyl (2E)-3-(dimethylamino)prop-2-enoate; With bis(1,1,1,5,5,5-hexafluoro-2,4-pentadionato)copper(II) hydrate; In 1,2-dichloro-ethane; at 60 ℃; for 4h; Inert atmosphere;

With trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201004073

Reference yield:

: 1257649-11-8
(Z)-ethyl 2-diazo-3-(methoxyimino)-3-(4-nitrophenyl)propanoate

: 999-59-7,20664-47-5
methyl (2E)-3-(dimethylamino)prop-2-enoate

: 1257649-36-7
3-ethyl 4-methyl 1-methoxy-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

: C₁₈H₂₃N₃O₇

Guidance literature:: With bis(1,1,1,5,5,5-hexafluoro-2,4-pentadionato)copper(II) hydrate; In 1,2-dichloro-ethane; at 60 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.201004073