(S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide

Base Information

Chemical Name:(S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide
CAS No.:1312613-69-6
Molecular Formula:C₂₃H₂₉N₃O₂
Molecular Weight:379.502
Hs Code.:

Synonyms:(S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide

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Chemical Property of (S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide

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Technology Process of (S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide

There total 3 articles about (S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1312613-66-3
(S)-(-)-N-(1-phenylethyl)-2-hydroxyimino-3-oxobutyramide

: 33103-90-1
N-methylidene adamantan-1-amine

: 1312613-69-6
(S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide

Guidance literature:: (S)-(-)-N-(1-phenylethyl)-2-hydroxyimino-3-oxobutyramide; N-methylidene adamantan-1-amine; With acetic acid; In ethanol; at 20 ℃; for 48h;

With hydrogenchloride; for 1.5h;

With sodium hydrogencarbonate; In methanol; chloroform; for 2h;
DOI:10.1016/j.tetasy.2011.04.005

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1312613-69-6
(S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 16 h / Reflux

2.1: acetic acid; sodium nitrite / water / Cooling with ice

3.1: acetic acid / ethanol / 48 h / 20 °C

3.2: 1.5 h

3.3: 2 h

With acetic acid; sodium nitrite; In ethanol; water; toluene;
DOI:10.1016/j.tetasy.2011.04.005

Reference yield:

: 63664-42-6
(S)-Phenylethyl Acetoacetamide

: 1312613-69-6
(S)-N-(1-phenylethyl)-1-(1-adamantyl)-5-methyl-3-oxido-1H-imidazole-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; sodium nitrite / water / Cooling with ice

2.1: acetic acid / ethanol / 48 h / 20 °C

2.2: 1.5 h

2.3: 2 h

With acetic acid; sodium nitrite; In ethanol; water;
DOI:10.1016/j.tetasy.2011.04.005