3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate

Base Information

• Chemical Name: 3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate
• CAS No.: 1613513-76-0
• Molecular Formula: C₂₁H₂₅Cl₂N₅O₃
• Molecular Weight: 466.367

Synonyms:3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate

Chemical Property of 3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate

Chemical Property:

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Technology Process of 3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate

There total 3 articles about 3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(1H-1,2,3-triazol-4-yl)butanoic acid → 3,5-dichlorobenzyl 8-azabicyclo[3.2.1]octan-3-ylcarbamate hydrochloride (1613513-78-2) + 3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate (1613513-76-0)

Guidance literature:

With triethanolamine; In N,N-dimethyl-formamide;

Reference yield:

hex-5-ynoic acid (53293-00-8) → 3,5-dichlorobenzyl 8-azabicyclo[3.2.1]octan-3-ylcarbamate hydrochloride (1613513-78-2) + 3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate (1613513-76-0)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium chloride / ethyl acetate; water; tert-butyl alcohol

2: ethanol

3: triethanolamine / N,N-dimethyl-formamide

With triethanolamine; sodium chloride; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

4-(1-Benzyl-1H-1,2,3-triazol-4-yl)butanoic acid → 3,5-dichlorobenzyl 8-azabicyclo[3.2.1]octan-3-ylcarbamate hydrochloride (1613513-78-2) + 3,5-Dichlorobenzyl (8-(4-(1H-1,2,3-triazol-4-yl)butanoyl)-8-azabicyclo[3.2.1]octan-3-yl)carbamate (1613513-76-0)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol

2: triethanolamine / N,N-dimethyl-formamide

With triethanolamine; In ethanol; N,N-dimethyl-formamide;

upstream raw materials:

hex-5-ynoic acid

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