(2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid

Base Information

Chemical Name:(2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid
CAS No.:124942-26-3
Molecular Formula:C₂₂H₃₃N₃O₆S₂
Molecular Weight:499.653
Hs Code.:

Synonyms:(2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid

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Chemical Property of (2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid

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Technology Process of (2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid

There total 3 articles about (2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 124921-79-5
(2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-4-oxo-5-azanonandisaeure

: 124942-26-3
(2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid

Guidance literature:: With borane; In tetrahydrofuran; for 24h; Ambient temperature;

Reference yield:

: (2S,8S)-2,8-Diamino-4-oxo-5-azanonandisaeure-bis(hydrobromid)

: 124942-26-3
(2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / 1 N NaOH / acetone / 5 h / pH 8.8

2: 97 percent / BH₃ / tetrahydrofuran / 24 h / Ambient temperature

With sodium hydroxide; borane; In tetrahydrofuran; acetone;

Reference yield:

: 124921-77-3
(2S,8S)-2,8-Bis(benzyloxycarbonylamino)-4-oxo-5-azanonadisaeure-dibenzylester

: 124942-26-3
(2S,8S)-2,8-Bis<(4-methylphenyl)sulfonylamino>-5-aza-1,9-nonandiol-hydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / HBr / acetic acid / 1) 30 min, room temperature, 2) 18 h, 50 deg C; or with Palladium/H₂

2: 67 percent / 1 N NaOH / acetone / 5 h / pH 8.8

3: 97 percent / BH₃ / tetrahydrofuran / 24 h / Ambient temperature

With sodium hydroxide; borane; hydrogen bromide; In tetrahydrofuran; acetic acid; acetone;