2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester

Base Information

Chemical Name:2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester
CAS No.:614751-52-9
Molecular Formula:C₂₂H₂₂N₂O₂
Molecular Weight:346.429
Hs Code.:

Synonyms:2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester

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Chemical Property of 2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester

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Technology Process of 2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester

There total 1 articles about 2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 614751-51-8
2-(2-bromo-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester

: 98-80-6
phenylboronic acid

: 614751-52-9
2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester

Guidance literature:: With tris(triphenylphosphano)palladium; sodium carbonate; In ethanol; toluene; Heating;
DOI:10.1016/S0960-894X(03)00594-8

Reference yield: 91.0%

: 614751-52-9
2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester

: 2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; Heating;
DOI:10.1016/S0960-894X(03)00594-8

Reference yield:

: 614751-52-9
2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid vinyl ester

: 2-(2-phenyl-pyridin-3-yl)-9-aza-bicyclo[4.2.1]non-2-ene-9-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / aq. HCl / dioxane / Heating

2: Et₃N / tetrahydrofuran; H₂O

With hydrogenchloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1016/S0960-894X(03)00594-8